Synthesis of New polymers of Triazole Derivatives

Reem Talal  Natheer; Asaad Khattab; Hana Mahmood

doi:10.56286/akzyww66

Synthesis of New polymers of Triazole Derivatives

Authors

Reem T. Natheer Department of Chemical Industries Techniques, Institute of Technical, Northern Technical University, Mosul, Iraq
Asaad F. Khattab Department of Chemistry, College of Science, University of Mosul, Mosul, Iraq
Hana Sh. Mahmood Department of Chemistry, College of Science, University of Mosul, Mosul, Iraq

DOI:

https://doi.org/10.56286/akzyww66

Keywords:

Triazole, Polymerazation, Heterocyclic compound, Thermal analysis , FTIR

Abstract

Thiatriazole is an important monomer, whereby it have two types of functional groups, amine and thiol. Within the frame of this work the triazole monomer have been prepared from its oxadiazole. Two type of polymers were prepared from this monomer via condensation with terephthaldehyde and succinyl chloride, whereby the binding units of the resulted polymers are differs, azomethine and amide respectively. Infrared spectroscopy and elemental analysis were used to identified the polymers. DTA, TGA and DSC analysis indicate the thermal history of the polymers. It was shown that polymer (1) was more flexibility than polymer (2) due to the lower Tg value due to the presence of azomethene group. The Tg are (138^oC) and (190^oC) respectively. Also the DTA, TGA indicates that polymer (2) have high thermal stability than polymer 1 due the presence of the amide group.

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Published

2024-10-08

Issue

Vol. 3 No. 3 (2024): Issue 3 (2024)

Section

Articles

License

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